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IBL-26-2701

Tocopherol-starch nanocomplex and functional beverages containing the same

Listed on
2026-10-19
Nanocomplex of tocopherol dispersed in water using starch and ultrasound without emulsifiers

This technology involves adding tocopherol, a fat-soluble vitamin, to a heated starch solution, followed by ultrasonic treatment and centrifugation to create a liquid tocopherol-starch nanocomplex that disperses evenly in water. No additives other than starch and water are used.

While tocopherol is highly effective for antioxidant activity, preventing atherosclerosis, and anti-aging, it is poorly water-soluble. When mixed with water, it tends to clump on the surface or stick to container walls, leading to significant loss and making product development difficult. Existing solubilization techniques often require organic solvents, emulsifiers, or surfactants, raising concerns about potential toxicity and limiting their use in food, beverages, cosmetics, and pharmaceuticals.

This technology works by having starch encapsulate tocopherol to form a complex, then using ultrasound to reduce particle size to the nano-to-submicron range, ensuring dispersion and storage stability. It can utilize natural starches like corn, potato, or rice, as well as various modified starches and tocopherol isomers, and can be produced through a simple process without expensive equipment. Applicable to antioxidant beverages, water-soluble vitamin E cosmetics, and oral nutritional supplements, it allows vitamin E—previously only oil-soluble—to be incorporated into clear aqueous solutions without loss, enhancing absorption in both ingestible and topical products.

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Key Features:
  • Heating a starch solution, adding and mixing tocopherol, and heating to obtain a tocopherol-starch mixture
  • Stirring and reacting the mixture at a high temperature, then cooling to room temperature to obtain a tocopherol-starch dispersion
  • Applying ultrasonic treatment to the tocopherol-starch dispersion to reduce particle diameter to a range of 100 nm to 1 μm
  • Centrifuging the ultrasonicated dispersion and collecting the supernatant to obtain a liquid tocopherol-starch nanocomplex

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Korea University
Seung-Taek Lim | Han-Gyeol Yoon
Document
Date of application:
2012-11-28
|
Patent registration number:
10-1460544
Industry
food•beverage
cosmetics
Technology
Food engineering
New materials
Country
Korea
Family Patent

N/A

Price
Price negotiable
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